Description

The price is for the base unit. To receive a commercial offer for the device in the working configuration, please contact the manager.

Liquid chromatograph “LUMACHROM®” with photometric / spectrophotometric / fluorimetric / spectrofluorimetric detection is designed for qualitative and quantitative determination of organic substances in complex samples by high performance liquid chromatography.
The block-modular principle allows you to create the optimal configuration of the device, depending on the tasks of the analytical laboratory – from routine to research.

The composition of the chromatograph “LUMACHROM®” includes:

  • base unit, consisting of a pump, a loop dosing valve, connecting elements;
  • detectors – photometric, spectrophotometric, fluorimetric and spectrofluorimetric.

Advantages:

  • the versatility of the liquid chromatograph lies in a wide choice of detection methods, increasing the information content of chromatographic analysis with the simultaneous use of 2 detectors, and also in compatibility with any type of HPLC detector;
  • block-modular principle allows creating an optimal configuration of a liquid chromatograph for solving specific user tasks;
  • Precise, pulse-free eluent flow is ideal for microcolumn HPLC;
  • chromatographic columns with an internal diameter of 2.1 mm of our own production minimize the cost of the mobile phase, increase the rapidity of the analysis, and reduce the cost of a single determination;
  • the possibility of completing a liquid chromatograph with columns and pre-columns of any size, both micro- and analytical scale, of our own and / or alternative production, is realized;
  • the independence of the modules allows them to be used as part of HPLC systems from other manufacturers;
  • modern computer programs provide the ability to automatically collect and process data with subsequent generation of a report in a user-friendly form;
  • the liquid chromatograph is accompanied by its own methodological support, while it is possible to adapt any existing and develop new HPLC methods;
  • quality and fast service is guaranteed throughout the territory of the Russian Federation and the CIS countries.

Additional features:

  • completion with any HPLC detector;
  • implementation of chromatographic analysis with the simultaneous use of two detectors of different types;
  • the use of micro- and analytical columns (with an inner diameter of 1; 2.1; 4; 4.6 mm);
  • connection of the column thermostat;
  • interchangeable loops for the dosing tap;
  • implementation of a gradient elution scheme;
  • use of fluorimetric and spectrofluorimetric detectors as liquid analyzers with the functions of a fluorimeter / spectrofluorimeter / photometer / spectrophotometer, etc. (for example, with a K-10 cuvette).

Areas of use

  • ecological and sanitary control;
  • control of safety and quality of food products and raw materials;
  • veterinary medicine, feed production;
  • pharmaceuticals;
  • criminology;
  • biochemistry;
  • clinical analysis.

Recommended scope of delivery:

  • base unit (pump, dosing tap, Hamilton syringe, test column, connecting elements);
  • optional detector: fluorimetric or spectrofluorimetric and/or photometric and/or spectrophotometric;
  • analysis kits (text of the methodology, standard sample, chromatographic column, pre-column, special reagents, light filters (for Fluorat-02-2M);
  • software “Multichrome” for fluorimetric, photometric and spectrophotometric detector, “PikExpert” – for spectrofluorimetric detector;
  • Personal Computer.

Installation conditions:

    • personal computer with installed OS Windows®-2000 and Windows®XP;
    • there should be no vibrations, sudden changes in ambient temperature, drafts, dust, strong magnetic and electric fields in the place where the chromatograph is installed;
    • the presence of a ground loop in the room for installing the chromatograph.

Specifications

base unit Syringe pump
“Lumachrom® N 1730”
Chamber volume 35 ml
Operating pressure up to 25 (50*) MPa
Programmable pressure limits (lower and upper) from 25 to 50* MPa
Automatic pressure relief up to 0.1 MPa
Operating range of space velocities of the mobile phase 1 – 1000 (2000*) µl/min
Loop valve,
Rheodyne® type
Dosing volume 10 µl (1*, 2*, 5* µl)
Detectors Fluorimetric filter
“Lumachrome FLD 2410 Fluorat®-02-2M”
Spectral range in the excitation channel 250 – 650 nm
Spectral range in the registration channel 250 – 650 nm
Detection limit: for anthracene** 2 ng/ml
Flow cell, working volume 1.5 μl
Spectrofluorimetric
“Lumahrom SFLD 2310 Fluorat®-02-Panorama”

(with programmable wavelength switching)
Spectral range of the monochromator in the excitation channel 210 – 670 nm
Spectral range of the monochromator in the registration channel 210 – 670 nm
Detection limit
for anthracene**
0.5 ng/ml
Flow cell, working volume 1.5 μl
Spectrophotometric
“Lumachrom® SFD 3220”
Operating wavelength range 190 – 360 nm
Wavelength Accuracy ±5 nm
Flow cell, optical path 10 mm
The width of the line no more than 20 nm
Detection limit for anthracene** 1 ng/ml
Photometric (single-wavelength)
“Lumachrome® FD 3120”
Wavelength 254 nm
Detection limit for anthracene** 1 ng/ml
Flow cell, optical path 10 mm
Data Acquisition and Chromatogram Processing System Fluorimetric,
Photometric,
Spectrophotometric
Software “Multichrome®” CJSC “Ampersend®”, Moscow
Spectrofluorimetric
detector
Software “PikExpert®” NPF AP LUMEX®, St. Petersburg

* on request

** dosing loop volume 10 µl

Liquid chromatograph Lumachrome allows to solve the following problems:

  • Determination of 2,4-D (pesticides) in drinking water
  • Determination of 5-hydroxymethylfurfural in fruit and vegetable and juice products, drinks, honey and dietary supplements
  • Determination of antibiotics of the tetracycline group in products of animal origin
  • Determination of aspartame, saccharin, caffeine and sodium benzoate in soft drinks
  • Determination of aflatoxin B1 in food products, raw materials and animal feed
  • Determination of aflatoxin M1 in milk and fermented milk products
  • Determination of benzo[a]pyrene in atmospheric air and air of the working area
  • Determination of benzo[a]pyrene in sources of air pollution (industrial emissions)
  • Determination of benzo[a]pyrene in food products, food raw materials and dietary supplements
  • Determination of benzo[a]pyrene in water samples
  • Determination of benzo[a]pyrene in samples of soils, soils, solid wastes and bottom sediments
  • Determination of vitamin K3 in premixes, vitamin concentrates and feed vitamin supplements
  • Determination of vitamins A, D and E in premixes and vitamin concentrates
  • Determination of vitamins A and E in premixes
  • Determination of vitamins A and E in samples of food products, food raw materials and dietary supplements
  • Determination of hesperidin and naringin in juice products
  • Determination of histamine in fish and fish products
  • Determination of deoxynivalenol in samples of food grains, flour and cereal products, animal feed and raw materials for their production
  • Determination of zearalenone in grain, products of its processing and in animal feed
  • Determination of preservatives and dyes in milk and dairy products according to GOST R 53752-2009
  • Determination of caffeine and theobromine in tea and tea products, coffee and coffee products, cocoa beans and cocoa products, dietary supplements
  • Determination of levomycetin (chloramphenicol) in products of animal origin
  • Determination of melamine in food products and raw materials for their production
  • Determination of melamine in food products and raw materials for their production
  • Determination of patulin in fruits and vegetables and dietary supplements
  • Determination of patulin in apple juice
  • Determination of sweeteners (acesulfame K, aspartame, saccharin), preservatives (sorbic, benzoic acids and their salts), caffeine in drinks
  • Determination of sweeteners in foods
  • Determination of sorbic and benzoic acids in processed fruits and vegetables
  • Determination of sorbic and benzoic acids and their salts in food products
  • Determination of phenol in the atmospheric air and the air of residential and public buildings
  • Determination of formaldehyde in indoor air
  • Determination of formaldehyde in water samples
  • Determination of С60, С70 and superheavy fullerenes in organic extracts
  • Determination of ochratoxin A in food products and food raw materials, dietary supplements, animal feed and raw materials for their production